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The graphite tube, the heart of the graphite furnace, plays a vital role in the overall stability of an analysis. In order to assure stable analytical conditions from one atomization cycle to the next, and from graphite tube to graphite tube, all graphite parts - contacts, tubes and platforms - must be subject to strict quality control by both the instrument manufacturer and the graphite manufacturer. PerkinElmer’s unique, transversely-heated graphite tube includes an integrated platform. The exceptionally uniform temperature distribution obtained with transverse heating significantly reduces or eliminates condensation of the sample matrix components and "memory” effects, and improves the atomization efficiency for refractory elements.
The tubes are compatible with PerkinElmer PinAAcle 900T, PinAAcle 900Z, AAnalyst 600, AAnalyst 800, Model 4100ZL, Model 4110ZL, Model 5100ZL, SIMAA 6000 Zeeman AA instruments.
|Product Brand Name||PerkinElmer|
|Product Group||THGA Graphite Tubes|
Toxic elements, such as lead (Pb) and cadmium (Cd), are entering the food chain through environmental contamination. Rice, as the most widely consumed cereal grain in Asia, can quickly pick up Pb and Cd from soil, thereby seriously endangering human health through diet. These toxic element levels need to be carefully monitored. Maximum levels of Pb and Cd are strictly regulated in Asian countries, especially in China; therefore, it is extremely important to develop a simple, reliable method for trace levels of Pb and Cd in rice. The allowable maximum levels of Pb and Cd in grains in EU and China are required to be below 0.2 mg/kg (Commission Regulation EC 1881/2006 and Chinese GB 2715-2016 Hygienic Standard). Graphite furnace atomic absorption spectroscopy (GFAAS) is the officially recommended technique for detection of trace elements in various food stuffs (GB/T 5009.15-2017, GB/T 5009. 12-2017 and EN 14083:2003). Food samples are usually pretreated before GFAAS analysis using various methods: microwave digestion, hot block digestion, dry ashing, and hot plate digestion. These conventional digestion procedures are usually complicated and time-consuming (2-4 hours or longer). Plus, they require large quantities of corrosive and oxidizing reagents, increasing the chance for contamination which could lead to inaccurate results. However, fast digestion can effectively speed up the sample preparation procedure while reducing the use of corrosive reagents and the chance for contamination.
Lead (Pb) and cadmium (Cd) are common pollutants in grains and are extremely toxic. Pb is harmful to human organs even at trace levels, and once it accumulates in the body, it causes inhibition of hemoglobin formation and neurological disorders. Cd is even classified as human carcinogen [Group 1 - according to International Agency for Research on Cancer]. It is reported that Cd leads to severe kidney problems which can be fatal and is also associated with brittle bones and liver problems. Rice, as the most widely consumed cereal grain in Asia/China, can quickly pick up Pb and Cd from toxins, pesticides and fertilizers in the soil, thereby endangering the health of millions of people through their diet. Therefore, it is extremely important to develop a simple, reliable method to monitor the levels of Pb and Cd in rice. According to Chinese national standard GB 2715-2016 Hygienic Standard for Grain, the maximum concentrations of Pb or Cd in grains must be below 0.2 mg/kg; the allowable level in the European Union is the same [EC 1881/2006]. The official technique for the determination of heavy metals in both cases is graphite furnace atomic absorption spectroscopy (GFAAS, GB/T 5009. 12-2017, GB/T 5009-2017. 15 and EN 14083:2003). Samples can be pretreated using various methods, including microwave digestion, hot block digestion, dry ashing, and hot plate digestion. It is found that these conventional digestion procedures are always complicated and time-consuming (two-four hours or even longer). Plus, conventional sample preparation techniques require large quantities of corrosive and oxidizing reagents, increasing the chance for contamination which could lead to inaccurate results. Special PTFE vessels are needed for microwave digestion; however, reusable utensils might also cause cross contamination.
PerkinElmer tubes are manufactured to the highest quality specifications. Our exclusive design ensures even heating over the entire length of the tube. Performance must be reproducible from day to day with respect to sensitivity; accuracy and precision. W
The production of high-quality graphite components for atomic absorption spectroscopy requires stringent quality control. To ensure high quality and consistency, a specific high-density base graphite material has been developed for use with PerkinElmer graphite furnace systems.