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  • Application Note

    Impurities in Lead with the Avio 500 ICP-OES Following London Metal Exchange Guidelines

    The London Metal Exchange issues specifications for a number of different metals in several grades. This work focuses on the analysis of lead of different purities with PerkinElmer’s Avio® 500 ICP Optical Emission Spectrometer (ICP-OES), using “Special Contract Rules for Standard Lead1” as a guideline for the analytes and concentrations.

  • Application Note

    Using MSF to Resolve Difficult Interferences in Metallurgical Samples with the Avio 500 ICP-OES

    The analysis of trace metals in metallurgical matrices also presents a challenge for ICP-OES: spectral interferences. Many elements have a large number of emission lines (i.e. approximately 20,000 for iron), which increases the potential for spectral interferences. This effect is compounded in metallurgical samples, where the matrix element(s) are present at high levels due to the minimal dilutions used.

  • Application Note

    Analysis of SiO2- and TiO2-Containing Medications Using ICP-OES Following USP 232/233 Guidelines with Software Designed to Aid in 21 CFR Part 11 Compliance

    This work demonstrates the ability of the Avio 200 ICP-OES to meet the USP <232>/<233> criteria for Class 1 and 2A elements in tablets containing TiO2 or SiO2 as excipients using Syngistix for ICP Enhanced Security software version 4.0 for 21 CFR Part 11 compliance.

  • Application Note

    Analysis of Wastewaters Following U.S. EPA 200.7 Using the Avio 500 ICP-OES

    This work focuses on the analysis of wastewaters following the guidelines provided in U.S. EPA Method 200.7. The U.S. Environmental Protection Agency (EPA) developed Method 200.7 for the determination of metals and trace elements in waters and wastes by ICP-OES, with the current version being Revision 4.4.1 While the scope of this method allows it to be applied to a variety of sample types, a common application is wastewater analysis.

  • Application Note

    Direct Analysis of Ethanol for Phosphorus, Sulfur, Copper, and Iron with the Avio 500 ICP-OES

    Ethanol is an important blending component in fuels commonly used in gasoline/petrol. Because of its wide use, it is important to monitor the concentrations of impurities in the ethanol which can negatively impact the performance of the resulting fuel. As a result, standards have been created for the phosphorus (P), sulfur (S), and copper (Cu) content in fuel.

    Ethanol analysis by ICP-OES can be challenging both due to volatility and high carbon content. However, with the right choice of sample introduction components and a robust plasma, ethanol can be measured with ease. This work demonstrates the ability of PerkinElmer’s Avio 500 ICP-OES to measure phosphorus, sulfur, copper, and iron in ethanol, leveraging the capabilities of Multicomponent Spectral Fitting (MSF) to eliminate the effect of interferences.

  • Brochure

    Refinery and Natural Gas Analysis

    Oil refineries and natural gas producers around the world require their lab operations to perform large numbers of analyses before their products are used in industries and by consumers. Detection of even the slightest impurities, accurate process control and hydrocarbon distribution analysis is critical to the success of these operations.That’s how PerkinElmer can help. As a global scientific leader and solutions provider to refining and natural gas labs, PerkinElmer's proven technology and experience meets the ever-changing needs of the oil and gas industry. PerkinElmer is committed to the success of your oil and gas sample analysis by providing the instrumentation, software, consumables, and services you need for fast, easy and precise testing. The result: better control of your operations and improved product quality.

  • Application Note

    Stable Analysis of Lithium Metaborate Fusion Samples with the Avio 500 ICP-OES

    The analysis of geological materials poses a challenge due to their matrix composition and the sample preparation process required to convert the samples into solution. A commonly used sample preparation technique for geological samples is lithium fusion, which involves mixing the sample with excess lithium borate and heating until the lithium borate melts and dissolves the sample to form a homogenous mass. The resulting solid is dissolved in acid for analysis.

    Fusion samples are some of the most punishing samples for an ICP-OES sample introduction system, as they contain high concentrations of Group I elements (such as lithium, sodium, and potassium), which can result in deposits on the nebulizer and injector, resulting in signal drift. In addition, the high concentrations of Group I elements may cause rapid devitrification of the quartz torch, so obtaining accurate results with good precision over longer time intervals is challenging. However, with the proper choice of sample introduction components, these challenges can be overcome.

    This work describes the analysis of fusion samples leveraging the PerkinElmer Avio® 500 ICP-OES, with a focus on long-term stability.

  • Application Note

    Analysis of In-Service Oils Following ASTM D5185 with the Avio 500 ICP-OES

    Globally, heavy machinery is used in construction, mining, and a variety of other areas. As the scale of the operations increase, the size, complexity, and cost of the equipment also increase, meaning that breakdowns can be costly, both in equipment repair and lost revenue. As a result, preventive maintenance is paramount. Lubricants are among the key fluids that can be tested, especially the oil used in engines. By monitoring the elemental concentration of the oil or other lubricants (hydraulics, transmission, gear), the status of that compartment can be determined.

  • Application Note

    Analysis of Allergy Medications Using ICP-OES Following USP 232/233 Guidelines with Software Designed to Aid in 21 CFR Part 11 Compliance

    This work demonstrates the ability of the Avio 500 ICP-OES to meet the USP <232>/<233> criteria for the analysis of orally-administered allergy tablets using Syngistix for ICP Enhanced Security software version 4.0, which provides the tools to help laboratories meet 21 CFR Part 11 compliance.

  • Flyer

    Laboratory Solutions for Lubricant Analysis

    Increasing demands for efficiency, productivity, data quality, and profitability pose ongoing challenges for lubricant testing laboratories, like yours, performing new lubricant or in-service oil analyses.

    Whether you need to achieve quick turnaround times, minimize downtime, or maximize lab efficiencies, you can rely on PerkinElmer as a trusted partner for simple-to-use and reliable testing solutions.

    Partnering with leading global standards organizations and hundreds of oil laboratories, we continually address laboratory needs and ever-changing standards while developing new methods and protocols that conform with ASTM®, regulatory, and customer-defined requirements.

    Download this infographic to learn more about our broad range of proven lubricant testing solutions.

  • Application Note

    Analysis of Oil Additives Following ASTM D4951 with the Avio 200 ICP-OES

    When blending base oils and additives for use as lubricants, it is important to know and control the concentrations of certain elements for optimal performance and longer engine life. This work will focus on the analysis of additives in new oils using PerkinElmer’s Avio™ 200 ICP Optical Emission Spectrometer (ICP-OES), which overcomes limitations of other ICP-OES systems and X-ray analyses.

  • Application Note

    A Novel Approach to Analysis of In-Service Lubricants for Particle Size/Count and Metal Content

    Particle counting is becoming a more routine tool for lubricant condition monitoring and maintenance programs to better identify particles of certain sizes and concentrations that can contribute to machine failure. In-service oils and other lubricants are monitored for particle size similarly to how they are monitored for elemental concentration. An increase in the ISO code (ISO 4406) for particle count or concentration of key wear metals indicates when maintenance is required.

    By adding the LPC 500 liquid particle counter in-line with the Avio 500 ICP-OES Oils system, lubricant samples can be analyzed for both wear metals and particles all in one run with results repeatably within one ISO code for the >4, >6 µm sizes for transmission and gear oil. Throughput of 45 seconds on average per sample with less than 1 mL is achieved for both ICP as well as particle counting and sizing, all with the smallest automated particle counting system in the lubricants testing industry.

    Download this application note to learn more.

  • Application Note

    Analysis of In-Service Oils Following ASTM D5185 with the Avio 200 ICP-OES

    With heavy machinery, it is important to assess its status during operation to prevent breakdowns and costly repairs. A key aspect is monitoring the status of the oil or lubricants used to lubricate various components such as engines, transmissions, gearboxes and many other important areas: if the oil degrades too much or becomes highly contaminated, it can damage various components. Because of its importance, ASTM created a method for the analysis of in-service oils: method D5185.

  • Application Note

    Compendium - Reliable Methods for Nutritional & Toxic Analysis of Breakfast Foods

    Breakfast is an important meal in providing essential nutrients to keep your energy levels up throughout the day. How do we ensure the food and beverages we consume are healthy, nutritious and safe? Following is a collection of application notes highlighting solutions that will help you identify micronutrients in milk, cereal, juice and fresh and dried fruits as well as toxic metals in tea, dairy products and apple juice to ensure safety of your breakfast foods.

  • Application Note

    High-Precision Analysis of Battery Materials with the Avio 500 ICP-OES

    Battery usage is growing rapidly as new uses are found, leading to the development of new battery types, technologies, and materials. Some commonly-used elements in different types of batteries include lithium, manganese, nickel, phosphorus, and zinc, among others. The percentage of these components can range from single digit up to 30%, depending on the battery.

    An important factor in obtaining optimum performance is accurately knowing the ratios of the major components, since deviations can negatively affect battery performance, as can the presence of impurities. Therefore, the major components must be measured both with high accuracy and precision, while, at the same time, measuring impurity levels.

    ICP-OES is the ideal analytical technique to meet these needs – it has a high tolerance to matrices, yet is capable of high precision and can accurately measure impurities down to the µg/L level. This work demonstrates the ability of PerkinElmer's Avio® 500 ICP-OES to achieve RSDs < 0.1% for matrix elements in simulated battery materials, the result of the instrument's ability to perform true simultaneous measurements.

    Download this application note to find out how the Avio 500 ICP-OES can measure elements with both high precision and accuracy while, at the same time, measuring common impurities.

  • Application Note

    Analysis of Impurities in Nickel with Avio 500 ICP-OES Following London Metal Exchange Guidelines

    The London Metal Exchange (LME) issues specifications for a variety of purities for different metals. This work focuses on the analysis of contaminants in nickel with PerkinElmer’s Avio® 500 ICP Optical Emission Spectrometer (ICP-OES), using “Special Contract Rules for Primary Nickel” as a guideline for the analytes and required concentrations.

  • Flyer

    OilPrep 4 Oil Diluter Flyer

    Need flexible sample preparation for wear metals and particle count analyses? The OilPrep 4 is a dedicated four-tip oil diluter that automatically dilutes oil samples with kerosene (V-Solv ICP solvent), in preparation for wear metals and particle counting/sizing analyses by inductively coupled plasma (ICP-OES) and single particle optical sizing (SPOS), such as with the Avio® ICP-OES and LPC 500™ Liquid Particle Counter.

    Some key benefits include:

    • • High throughput – Significantly improves productivity and efficiency versus manual or single-tip systems. Diluting up to 250 samples per hour, one OilPrep 4 oil diluter can prepare approximately 2000 samples in 8 hours.
    • • Flexibility – Innovative Varispan® technology provides automatic computer-controlled variable sample probe spacing for multi-tipped processing of original sample containers.
    • • Time Savings – Unlike alternate technologies, PerkinElmer’s Ultrasonic Liquid Level Sensing is not impacted by individual sample viscosities, color, or external lighting.

    Download the flyer to discover more.

  • Brochure

    Avio 200 Inductively Coupled Plasma Optical Emission Spectrometer

    Capable of handling even the most difficult, high-matrix samples without dilution, PerkinElmer’s Avio® 200 hybrid-scanning system brings a whole new level of performance and flexibility to ICP. What's more, that unprecedented performance comes with unparalleled ease-of-use. Unique hardware features and the industry’s most intuitive software combine to make multi-element measurements as easy as single-element analyses.

    The smallest ICP on the market, Avio 200 offers efficient operation, reliable data, and low cost of ownership by delivering:

  • The lowest argon consumption of any ICP
  • The fastest ICP startup (spectrometer ready in just minutes from power on)
  • Superior sensitivity and resolution for all elements of interest
  • Extended linear range with dual viewing technology
  • Download the brochure to learn more about the unique capabilities and benefits of PerkinElmer's Avio 200 hybrid-scanning ICP-OES.

  • Brochure

    Avio 500 ICP Optical Emission Spectrometer

    With a truly simultaneous system, high sensitivity and superior resolution, the Avio® 500 ICP-OES helps your lab accomplish more — even with the most difficult samples — while making the most of your resources.

    The Avio 500 provides:

    1. Unsurpassed matrix tolerance with vertical torch design
    2. Lowest argon consumption of any ICP — at least 50% lower than other systems
    3. Simultaneous background correction for faster sample-to-sample time and improved data accuracy
    4. High throughput enabled by dual view technology, simultaneous data acquisition and low routine maintenance
    5. Maximized instrument run time with Radian Remote Monitoring

    With the Avio 500 ICP-OES, you can do more — faster and more easily. Now is the time to expand your range and extend your resources. Now is the time for the Avio 500 ICP-OES.

    Download the brochure to learn more.

  • Application Note

    Analysis of Impurities in Aluminum with the Avio 200 ICP-OES Following London Metal Exchange Guidelines

    Due to aluminum’s varied uses and popularity, there are many grades available. The London Metal Exchange (LME) lists specifications for two commonly-used aluminum (Al) purities: 99.5% and 99.7%1, with each having up to six inorganic impurities specified. ICP-OES is the best technique for measuring these impurities at these levels due to its ability to easily handle high-matrix samples and simplicity of operation.

    This work describes the analysis of impurities in Al at the LME specifications using the Avio® 200 hybrid scanning ICP-OES, an ideal choice for this application – its optical design provides excellent light throughput, essential for measuring lower concentrations with shorter analytical times, plus, its charge-coupled device (CCD detector) provides simultaneous background and analyte measurement, important for samples such as metal matrices.

  • Application Note

    Analysis of Aluminum Alloys with the Avio 200 ICP-OES Following London Metal Exchange Guidelines

    Due to its unique characteristics, aluminum (Al) is used in a wide variety of commercial and industrial applications. Its utility can be further enhanced by combining it with other metals to create aluminum-based alloys, where the non-aluminum additives can make up to 15% of the total alloy, by weight.

    Because of its popularity and multiple compositions, the London Metal Exchange (LME) lists four different specifications for Al alloy compositions. In these specifications, silicon, copper, zinc, and iron are considered major additions, as they are mostly greater than 1% composition by weight. Therefore, these four elements must be determined with greater accuracy (± 2%) than the others.

    This work describes the determination of additives to Al in aluminum alloys at the LME specifications using the Avio® 200 hybrid scanning ICP-OES, an ideal choice for labs performing this application thanks to its charge-coupled device (CCD) detector, providing simultaneous background and analyte measurement, important when dealing with complex matrices, such as alloys.

  • Application Note

    Analysis of Micronutrients in Milk Using the Avio 200 ICP-OES

    With its great importance, milk is available in several different forms: fresh, boxed (ultraheat treated), powdered, and evaporated. The most commonly consumed form varies globally, being dependent on factors such as geography, culture, and climate. For milk producers, internal quality control and the possibility of external monitoring provide strong incentives for the ability to quickly, accurately, and easily monitor nutrients in their products.

  • Application Note

    Meeting the Challenges of Soil Analysis with the Avio 200 ICP-OES

    The analysis of soils for elemental contents presents challenges during the sample preparation step. A common method for preparing a soil sample for inorganic elemental analysis involves digesting the soil sample in an acid that is heated to near-boiling to extract the elements for analysis. When using open vessels in heating blocks, this extraction method typically takes four hours or more to complete. The sample must then be centrifuged or filtered to remove solid particles prior to analysis. The use of a microwave digestion system can speed this up significantly by completing the acid digestion in less than 50 minutes.

  • FAQ

    Syngistix for ICP Enhanced Security Software for Laboratories Subject to 21 CFR Part 11 Regulations

    The regulations of 21 CFR Part 11 cover overall system compliance and include administrative, procedural and technical elements. Software alone cannot be compliant without the development and implementation of the other elements. PerkinElmer’s Syngistix™ for ICP Enhanced Security™ software for Avio® and Optima® ICP-OES systems provides features that, when coupled with appropriate policies and procedure, fulfill the requirements for closed-system electronic records in 21 CFR Part 11. Syngistix Enhanced Security software also fulfills the elements relating to electronic signatures.